Agilent SuperNova Dual Source diffractometer with an Atlas detector | 2409 independent reflections |
Radiation source: fine-focus sealed tube | 2109 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.022 |
Detector resolution: 5.3048 pixels mm-1 | θmax = 69.1°, θmin = 6.3° |
ω scan | h = −8→7 |
Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014) | k = −8→8 |
Tmin = 0.737, Tmax = 0.812 | l = −17→16 |
7634 measured reflections |