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. 2017 Jan 1;73(Pt 1):88–91. doi: 10.1107/S2056989016020156
Bruker APEXII CCD diffractometer 17956 independent reflections
Radiation source: fine-focus sealed tube 10069 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.156
Detector resolution: 8.3333 pixels mm-1 θmax = 30.6°, θmin = 1.5°
φ and ω scans h = −14→14
Absorption correction: multi-scan (SADABS; Bruker, 2013) k = −10→10
Tmin = 0.81, Tmax = 0.99 l = −57→57
76791 measured reflections