| Bruker APEXII CCD diffractometer | 17956 independent reflections |
| Radiation source: fine-focus sealed tube | 10069 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.156 |
| Detector resolution: 8.3333 pixels mm-1 | θmax = 30.6°, θmin = 1.5° |
| φ and ω scans | h = −14→14 |
| Absorption correction: multi-scan (SADABS; Bruker, 2013) | k = −10→10 |
| Tmin = 0.81, Tmax = 0.99 | l = −57→57 |
| 76791 measured reflections |