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. 2016 Dec 27;2016:5890897. doi: 10.1155/2016/5890897

Table 2.

Fractional factorial design (FFD) model totalizing 11 experiments aiming at the optimization of trans-resveratrol extraction in mg/g extract, by the microwave-assisted technique.

Entry St (rpm) T (°C) Solvent concentration
(MeOH aq.) (%)
Mass : solvent proportion (g/mL) Content of t-resveratrol
(mg/g extract)a
1 −1 (600) −1 (30) −1 (60) −1 (1 : 60) 0.235
2 1 (1200) −1 (30) −1 (60) 1 (1 : 20) 0.786
3 −1 (600) 1 (70) −1 (60) 1 (1 : 20) 0.075
4 1 (1200) 1 (70) −1 (60) −1 (1 : 60) 0.456
5 −1 (600) −1 (30) 1 (100) 1 (1 : 20) 0.231
6 1 (1200) −1 (30) 1 (100) −1 (1 : 60) 0.085
7 −1 (600) 1 (70) 1 (100) −1 (1 : 60) 0.103
8 1 (1200) 1 (70) 1 (100) 1 (1 : 20) 0.289
9 0 (900) 0 (50) 0 (80) 0 (1 : 40) 0.143
10 0 (900) 0 (50) 0 (80) 0 (1 : 40) 0.117
11 0 (900) 0 (50) 0 (80) 0 (1 : 40) 0.124

aMeasured by HPLC-DAD.