Table 2.
Fractional factorial design (FFD) model totalizing 11 experiments aiming at the optimization of trans-resveratrol extraction in mg/g extract, by the microwave-assisted technique.
| Entry | St (rpm) | T (°C) | Solvent concentration (MeOH aq.) (%) |
Mass : solvent proportion (g/mL) | Content of t-resveratrol (mg/g extract)a |
|---|---|---|---|---|---|
| 1 | −1 (600) | −1 (30) | −1 (60) | −1 (1 : 60) | 0.235 |
| 2 | 1 (1200) | −1 (30) | −1 (60) | 1 (1 : 20) | 0.786 |
| 3 | −1 (600) | 1 (70) | −1 (60) | 1 (1 : 20) | 0.075 |
| 4 | 1 (1200) | 1 (70) | −1 (60) | −1 (1 : 60) | 0.456 |
| 5 | −1 (600) | −1 (30) | 1 (100) | 1 (1 : 20) | 0.231 |
| 6 | 1 (1200) | −1 (30) | 1 (100) | −1 (1 : 60) | 0.085 |
| 7 | −1 (600) | 1 (70) | 1 (100) | −1 (1 : 60) | 0.103 |
| 8 | 1 (1200) | 1 (70) | 1 (100) | 1 (1 : 20) | 0.289 |
| 9 | 0 (900) | 0 (50) | 0 (80) | 0 (1 : 40) | 0.143 |
| 10 | 0 (900) | 0 (50) | 0 (80) | 0 (1 : 40) | 0.117 |
| 11 | 0 (900) | 0 (50) | 0 (80) | 0 (1 : 40) | 0.124 |
aMeasured by HPLC-DAD.