Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.
Solvent screening for decarboxylative coupling in aqueous media
| Entry | Ratio H2O/MeCN | Ratio TIQ/alkyne | Yield 17/% |
|---|---|---|---|
| 1 | 100:0 | 2:1 | Traces |
| 2 | 99:1 | 2:1 | Traces |
| 3 | 90:10 | 2:1 | Traces |
| 4 | 50:50 | 2:1 | Traces |
| 5 | 100:0 | 1:1 | Traces |
| 6 | 99:1 | 1:1 | 5a |
| 7 | 90:10 | 1:1 | 50b |
| 8 | 50:50 | 1:1 | 80b |
aGC yield with dodecane as internal standard
bIsolated yield
