. Author manuscript; available in PMC: 2018 Feb 15.

Published in final edited form as: Anal Chim Acta. 2016 Dec 10;954:140–150. doi: 10.1016/j.aca.2016.12.003

Table 3.

Linear calibration curves (area = slope x [μg mL⁻¹] + intercept), limits of detection (LOD), limits of quantification (LOQ) and repeatability of measurements for different representative lipid classes.

Lipid Class	Range of linearity (μg mL⁻¹)	Slope	Intercept	R²	LOD (μg mL⁻¹)	LOQ (μg mL⁻¹)	Repeatability (%)^a
Lipid Class	Range of linearity (μg mL⁻¹)	Slope	Intercept	R²	LOD (μg mL⁻¹)	LOQ (μg mL⁻¹)	Retention times	Peak areas
TG	30–750	12.407	−1622.3	0.9915	72.80	220.60	2.59	7.91
Cholesterol	30–300	19.872	−776.77	0.9901	44.58	135.10	0.66	4.47
1,2-DG	30–300	13.086	−252.04	0.9915	37.39	124.65	1.01	5.81
FA C18:1	30–300	18.522	−652.89	0.9911	42.33	128.27	1.18	6.19
CL	150–1500	9.1791	−732.37	0.9930	140.52	425.82	0.26	6.89
PE	60–1200	7.524	−462.79	0.9988	27.35	82.88	0.06	2.38
PI	45–1800	8.1921	−325.31	0.9957	77.69	235.43	0.04	5.11
PC	75–1500	9.7677	−728.84	0.9971	53.00	160.60	0.14	4.15
SM	150–1500	9.4956	−1044.1	0.9907	85.94	260.42	0.03	2.99

Standard deviations based on six consecutive measurements.