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. Author manuscript; available in PMC: 2017 Jan 24.
Published in final edited form as: J Am Chem Soc. 2016 Dec 29;139(1):119–129. doi: 10.1021/jacs.6b03512

Figure 11.

Figure 11

Detection of a green metastable intermediate in the reaction between (Pr,Pr)Fe(III) (2) and 10 equiv of IBX-ester at −73 °C in MeOH to form sulfenate 5 over the course of 36 min.