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Stepwise MOF formation observed in situ. (a) Synthesis of ZIFs49,56 and (b) Zn-MOF-74, with images of the milling jar for each step.57 (c) Discovery of katsenite phase: time-resolved diffractogram with highlighted periods of existence of ZIF-8, kat, and dia frameworks.14 Symbol for mechanochemical reactivity in panels a and b proposed by Rightmire et al.5
