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. Author manuscript; available in PMC: 2017 Aug 1.
Published in final edited form as: Adv Healthc Mater. 2016 Apr 25;5(15):1868–1873. doi: 10.1002/adhm.201600230

Table 1.

Summary of synthesized polymer prodrugs [a]

Entry Molar feed ratioCarb-PTX: TMC: I DPCarb-PTX: TMC Yield% Mng mol−1 Mw/Mn
mPEG-polyPTX8.3 10: 0: 1 8.7: 0 81 14900 1.05
mPEG-polyPTX5.8 6: 0: 1 5.8: 0 80 11600 1.08
mPEG-poly(TMC-PTX2.7) 3: 15: 1 2.7: 14.8 82 9600 1.12
mPEG-poly(TMC-PTX1.3) 2: 15: 1 1.4: 14.2 80 8000 1.10
[a]

I is mPEG (Mn of 5 kDa). The DP was calculated by 1H NMR in CDCl3. The Mn and Mw/Mn were obtained from GPC-MALLS in tetrahydrofuran. The polymerization was carried out in dichloromethane at room temperature using TU and DBU as co-catalysts.