Table 1.
Determination number | Potassium hydrogen phthalatea | Potassium hydrogen phthalateb | Benzoic acida | Benzoic acidb | Hydrochloric acida c | Adipic acida d | Adipic acidb e | Sodium carbonatea |
---|---|---|---|---|---|---|---|---|
assay | assay | assay | assay | assay | assay | assay | assay | |
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|
% | % | % | % | % | % | % | % | |
1 | 99.976 | 99.979 | 99.985 | 99.991 | 99.982 | 99.935 | 99.985 | 99.909 |
2 | 99.980 | 99.976 | 99.991 | 99.993 | 100.004 | 99.937 | 99.987 | 99.901 |
3 | 99.978 | 99.981 | 99.989 | 99.996 | 100.014 | 99.937 | 99.980 | 99.915 |
4 | 99.970 | 99.976 | 100.001 | 99.991 | 100.003 | 99.947 | 99.981 | 99.910 |
5 | 99.974 | 99.974 | 99.985 | 99.986 | 100.002 | 99.942 | 99.989 | 99.920 |
6 | …………………………………… | …………………………………… | …………………………………… | 99.998 | 99.999 | 99.955 | …………………………………… | …………………………………… |
7 | …………………………………… | …………………………………… | …………………………………… | …………………………………… | 99.990 | 99.951 | …………………………………… | …………………………………… |
8 | …………………………………… | …………………………………… | …………………………………… | …………………………………… | …………………………………… | 99.948 | …………………………………… | …………………………………… |
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Mean | 99.976 | 99.977 | 99.990 | 99.994 | 99.999 | 99.945 | 99.984 | 99.911 |
Standard deviation | 0.004 | 0.003 | 0.006 | 0.004 | 0.010 | 0.007 | 0.004 | 0.007 |
Timed by electric clock.
Timed by time interval meter.
Assay based on calculated acidity by the pressure-distillation method.
Once recrystallized from melt.
Twice recrystallized from melt.