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. 1959 Oct 1;63A(2):153–159. doi: 10.6028/jres.063A.008

Table 1.

Summary of results

Determination number Potassium hydrogen phthalatea Potassium hydrogen phthalateb Benzoic acida Benzoic acidb Hydrochloric acida c Adipic acida d Adipic acidb e Sodium carbonatea
assay assay assay assay assay assay assay assay









% % % % % % % %
1   99.976   99.979     99.985   99.991     99.982   99.935   99.985   99.909
2   99.980   99.976     99.991   99.993   100.004   99.937   99.987   99.901
3   99.978   99.981     99.989   99.996   100.014   99.937   99.980   99.915
4   99.970   99.976   100.001   99.991   100.003   99.947   99.981   99.910
5   99.974   99.974     99.985   99.986   100.002   99.942   99.989   99.920
6 …………………………………… …………………………………… ……………………………………   99.998     99.999   99.955 …………………………………… ……………………………………
7 …………………………………… …………………………………… …………………………………… ……………………………………     99.990   99.951 …………………………………… ……………………………………
8 …………………………………… …………………………………… …………………………………… …………………………………… ……………………………………   99.948 …………………………………… ……………………………………








Mean   99.976   99.977     99.990   99.994     99.999   99.945   99.984   99.911
Standard deviation     0.004     0.003    0.006     0.004    0.010     0.007     0.004     0.007
a

Timed by electric clock.

b

Timed by time interval meter.

c

Assay based on calculated acidity by the pressure-distillation method.

d

Once recrystallized from melt.

e

Twice recrystallized from melt.