Four pyrrole derivatives used as building blocks in the synthesis of minor-groove binders

. 2017 Jan 27;73(Pt 2):254–259. doi: 10.1107/S2056989017001177

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
O1	0.0269 (7)	0.0263 (7)	0.0346 (8)	0.0097 (6)	0.0057 (6)	−0.0033 (6)
O2	0.0338 (7)	0.0252 (8)	0.0452 (9)	−0.0027 (6)	0.0168 (6)	0.0024 (6)
O3	0.0375 (7)	0.0232 (7)	0.0167 (6)	−0.0023 (6)	0.0043 (5)	0.0010 (5)
N1	0.0191 (7)	0.0147 (7)	0.0207 (7)	−0.0002 (6)	−0.0014 (5)	0.0014 (6)
N2	0.0192 (7)	0.0228 (8)	0.0260 (8)	0.0025 (6)	0.0024 (6)	0.0007 (6)
N3	0.0244 (7)	0.0187 (7)	0.0173 (7)	0.0031 (6)	0.0043 (6)	0.0003 (6)
N4	0.0286 (9)	0.0492 (12)	0.0484 (12)	−0.0016 (8)	−0.0035 (8)	0.0092 (9)
C1	0.0184 (8)	0.0180 (9)	0.0219 (9)	0.0033 (7)	−0.0015 (6)	−0.0014 (7)
C2	0.0158 (7)	0.0198 (9)	0.0205 (8)	0.0023 (7)	−0.0003 (6)	0.0008 (7)
C3	0.0183 (8)	0.0174 (9)	0.0213 (9)	0.0002 (7)	−0.0013 (6)	0.0004 (7)
C4	0.0191 (8)	0.0158 (8)	0.0171 (8)	−0.0001 (7)	−0.0022 (6)	0.0004 (6)
C5	0.0265 (9)	0.0162 (8)	0.0211 (9)	−0.0021 (7)	0.0011 (7)	0.0033 (7)
C6	0.0256 (9)	0.0240 (10)	0.0235 (9)	−0.0056 (8)	−0.0015 (7)	0.0044 (8)
C7	0.0317 (10)	0.0356 (11)	0.0253 (10)	−0.0127 (9)	0.0031 (8)	0.0041 (9)
C8	0.0592 (15)	0.0333 (12)	0.0448 (14)	−0.0203 (11)	0.0108 (11)	0.0026 (10)
C9	0.0332 (12)	0.0749 (19)	0.0469 (14)	−0.0221 (12)	−0.0010 (10)	0.0124 (13)
C10	0.0171 (8)	0.0205 (9)	0.0177 (8)	−0.0029 (7)	−0.0020 (6)	−0.0020 (7)
C11	0.0260 (9)	0.0221 (9)	0.0219 (9)	0.0049 (7)	0.0019 (7)	−0.0042 (7)
C12	0.0287 (10)	0.0318 (11)	0.0307 (11)	0.0028 (8)	0.0056 (8)	−0.0027 (8)
C13	0.0281 (10)	0.0359 (11)	0.0314 (11)	−0.0020 (9)	0.0011 (8)	−0.0004 (9)
C14	0.0435 (14)	0.076 (2)	0.0645 (18)	−0.0022 (14)	−0.0170 (13)	0.0193 (15)
C15	0.0366 (13)	0.074 (2)	0.079 (2)	−0.0156 (13)	−0.0038 (13)	0.0177 (16)