| Oxford Diffraction Xcalibur E diffractometer | 4852 independent reflections |
| Radiation source: fine-focus sealed tube | 3295 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.038 |
| ω scans | θmax = 27.0°, θmin = 3.3° |
| Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2010) | h = −14→14 |
| Tmin = 0.828, Tmax = 1.000 | k = −21→20 |
| 14949 measured reflections | l = −15→15 |
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