Skip to main content
. 2016 Oct 28;12(2):106–119. doi: 10.1002/cmdc.201600441

Scheme 2.

Scheme 2

Synthesis of compound 10. Reagents and conditions: a) (2‐((dimethylamino)methyl)phenyl)magnesium bromide, THF, RT, 2 h, 72.1–83.8 %; b) TBAP/NMO, 1,4‐dioxane, RT, 15 h, 77.2–87.5 %; c) Grignard reagent, THF, RT, 2 h, 38.1–56.2 %.