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. 2017 Jan 25;13:164–173. doi: 10.3762/bjoc.13.19

Scheme 7.

Scheme 7

Attempted synthesis of hexasaccharide repeating unit 36 via a convergent [3 + 3] glycosylation strategy and exploratory control experiments. A) Failed [3 + 3] glycosylation; B) failed model [1 + 3] glycosylation; C) low yielding model coupling of two monosaccharides.