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. 2016 Sep 19;44(2):95–107. doi: 10.1007/s00269-016-0840-7

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© The Author(s) 2016

Open AccessThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.

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Fig. 1 — Rietveld plot for meta-alunogen obtained from alunogen by storage at dry conditions (0 % RH). Peak positions permitted by unit-cell metric are indicated by tick marks (middle portion). Residuals of the Rietveld refinement are R _wp = 13.59 %, R _Bragg = 2.45 % and GoF = 2.68