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. Author manuscript; available in PMC: 2018 Jan 27.
Published in final edited form as: J Nat Prod. 2016 Dec 20;80(1):96–107. doi: 10.1021/acs.jnatprod.6b00744

Table 4.

13C NMR Data of Compounds 1–12 at 125 MHz

No. 1a 2a 3a 4a 5a 6b 7a 8a 9b 10b 11a 12a
1 25.7 26.1 26.1 26.0 26.0 27.3 26.1 28.2 30.4 34.3 28.5 28.6
2 16.0 16.1 16.1 8.3 8.3 9.0 16.0 14.3 10.0 11.7 15.8 15.8
3 24.8 24.9 25.0 27.5 27.9 28.4 24.9 23.9 28.4 25.9 26.6 26.7
4 142.4 142.6 142.6 90.8 90.7 91.3 141.3 138.0 89.9 146.1 151.3 151.3
5 131.5 132.2 132.2 158.7 158.9 159.5 132.8 155.8 161.0 43.8 135.4 135.4
6 40.7 41.1 41.1 127.1 127.0 129.2 41.9 115.7 126.8 44.6 151.4 151.4
7 131.2 131.1 131.0 143.2 143.3 132.6 134.8 124.8 154.6 153.3 129.7 129.7
8 200.2 200.2 200.0 198.8 198.4 200.6 204.1 104.7 105.2 108.0 197.0 197.1
9 80.5 80.1 80.1 77.9 77.8 78.7 80.6 75.9 78.8 80.0 83.2 83.2
10 51.3 51.1 51.2 50.3 50.2 51.5 50.4 49.3 50.5 47.4 57.6 57.6
11 148.1 147.5 147.6 129.0 128.8 141.5 144.2 153.8 125.3 133.2 65.3 65.4
12 170.5 171.8 171.2 170.3 170.5 172.3 169.4 171.8 173.2 173.2 172.0 172.0
13 20.8 20.5 20.5 21.4 21.4 21.0 19.2 10.4 10.6 10.7 18.9 19.1
14 15.2 15.5 15.6 15.5 15.5 16.1 15.5 14.5 14.3 22.7 14.9 14.9
15 25.4 25.4 25.4 36.9 36.8 36.8 25.4 121.0 36.1 112.5 29.3 29.2
1′ 25.6 25.7 25.7 27.9 27,5 27.4 26.2 25.6 28.2 26.6 26.6 26.6
2′ 12.0 12.0 12.0 10.2 10.2 16.9 11.8 11.2 11.0 11.4 10.3 10.4
3′ 28.0 28.4 28.6 29.3 29.0 24.1 27.2 29.2 30.4 29.8 29.8 29.7
4′ 77.3 77.3 77.5 77.3 77.1 49.4 77.3 77.3 78.1 78.4 79.0 78.8
5′ 61.0 59.9 59.8 54.6 54.0 54.5 61.8 55.8 53.1 57.1 55.7 56.5
6′ 23.4 22.3 22.2 22.0 22.8 26.2 25.3 21.7 22.5 24.9 27.8 27.8
7′ 171.9 168.5 168.5 166.3 170.3 170.0 174.4 171.6 173.9 173.2 59.1 59.1
8′ 93.3 93.5 93.7 87.7 87.6 88.8 93.3 85.9 87.5 92.0 95.6 95.5
9′ 55.9 55.1 55.1 52.7 52.8 52.4 55.0 55.5 52.1 54.0 52.2 52.1
10′ 44.9 44.8 44.9 45.1 45.0 45.7 44.7 47.8 46.0 46.5 43.0 43.1
11′ 123.6 127.5 127.4 128.6 125.3 129.5 123.2 123.6 124.7 128.4 145.9 146.1
12′ 171.4 172.4 172.5 172.9 171.6 174.9 171.9 171.8 173.4 173.9 168.4 168.4
13′ 55.8 54.8 54.9 55.1 55.8 54.5 55.2 55.3 56.6 54.6 123.1 129.7
14′ 26.6 26.4 26.4 24.4 24.3 23.1 26.2 25.3 24.5 25.8 24.0 24.0
15′ 72.4 70.5 70.1 69.8 69.1 64.1 72.2 68.3 69.3 72.4 69.5 70.4
1″ 165.5 166.1 166.8 166.0 166.3 166.2 167.0 168.4 168.3 167.9 166.0
2″ 135.4 114.9 115.4 115.2 114.5 113.0 113.4 114.4 114.1 128.2 114.3
3″ 151.2 153.4 158.8 153.9 160.9 153.9 159.1 159.9 160.1 138.7 154.2
4″ 195.1 67.4 27.6 67.9 67.1 66.2 67.2 67.2 67.3 14.7 67.3
5″ 11.0 15.9 20.6 16.1 15.8 15.9 16.0 16.0 15.8 12.3 16.0
6″ 173.2 171.8 171.9 173.3 172.2 174.8 174.8 171.7
7″ 28.7 28.8 28.9 28.6 29.5 28.5 173.9 28.9
8″ 28.7 29.0 29.1 28.7 29.2 28.5 29.5 29.0
9″ 172.1 173.0 173.0 172.1 172.9 171.9 29.5 172.9
12-OMe 52.8 52.9 52.9 53.0 53.1 53.1 53.0 52.2 52.1
6″-OMe 52.2 52.3 53.0 52.6
9″-OMe 52.1 52.2 52.1
a

Data were measured in CDCl3 and

b

data were measured in CD3OD.