Table 1.
Crystal data.
| Chemical formula | C30H24CuN2O8·2(C2H6O) |
| M r | 696.19 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 150 |
| a, b, c (Å) | 9.745 (4), 12.979 (5), 12.375 (5) |
| β (°) | 94.206 (7) |
| V (Å3) | 1561.0 (11) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.76 |
| Crystal size (mm) | 0.41 × 0.15 × 0.04 |
| Absorption correction | Multi-scan SADABS v20012/1, Sheldrick, G. M., (2012) |
| T min, Tmax | 0.613, 0.745 |
| Number of measured, independent, and observed [I > 2σ(I)] reflections | 12319, 2757, 1590 |
| R int | 0.129 |
| R[F2 > 2σ(F2)], wR(F2), S | 0.062, 0.169, 1.01 |
| Number of reflections, number of parameters | 2757, 218 |
| Δ〉max, Δ〉min (e Å−3) | 0.36, −0.39 |