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. 2017 Feb 19;2017:7895023. doi: 10.1155/2017/7895023

Table 1.

Crystal data.

Chemical formula C30H24CuN2O8·2(C2H6O)
M r 696.19
Crystal system, space group Monoclinic, P21/c
Temperature (K) 150
a, b, c (Å) 9.745 (4), 12.979 (5), 12.375 (5)
β (°) 94.206 (7)
V3) 1561.0 (11)
Z 2
Radiation type Mo
μ (mm−1) 0.76
Crystal size (mm) 0.41 × 0.15 × 0.04
Absorption correction Multi-scan 
SADABS v20012/1, Sheldrick, G. M., (2012)
T min, Tmax 0.613, 0.745
Number of measured, independent, and observed [I > 2σ(I)] reflections 12319, 2757, 1590
R int 0.129
R[F2 > 2σ(F2)], wR(F2), S 0.062, 0.169, 1.01
Number of reflections, number of parameters 2757, 218
Δ〉max, Δ〉min (e Å−3) 0.36, −0.39