Table 1.
Scaling Statistics Between the 2DYR and 3WG7 Data Sets
| Single‐Crystal/2DYR | XFEL/3WG7 | |
|---|---|---|
| Unit cell (P212121) | ||
| a (Å) | 182.59 | 182.60 ± 0.38 |
| b (Å) | 205.14 | 204.51 ± 0.55 |
| c (Å) | 178.25 | 178.29 ± 0.46 |
| Resolution (Å) | 1.80 Å | 1.90Å |
| Number of crystals | Not available | 76 crystals/1,107 still images |
| Intensity R merge | Not available | 0.243 |
| Number of reflections | 607,319 | 473,986 |
| R work | 0.202 | 0.195 |
| R free | 0.227 | 0.230 |
| Isomorphous differences as a function of scaling procedures | ||
| R iso (all) | 0.202 (Intensity R iso = 0.341) | |
| R iso (4.50–1.89 Å) | 0.183 (Intensity R iso = 0.303) | |
| R iso (140–4.50 Å) | 0.205 (Intensity R iso = 0.394) | |
| R iso (second pass) | 0.185 (Intensity R iso = 0.331) | |
| Statistics for refinement of models for this analysis | ||
| R work | 0.131 | 0.168 |
| R free | 0.168 | 0.218 |