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. Author manuscript; available in PMC: 2017 Dec 7.
Published in final edited form as: J Am Chem Soc. 2016 Nov 28;138(48):15559–15562. doi: 10.1021/jacs.6b09657

Scheme 3.

Scheme 3

Generation and Decomposition of the Diazosulfide 5.a

aSpectroscopic data shown corresponds to the major diazosulfide isomer. Reaction was run under air. 1H NMR data were acquired at −20 °C.