| Crystal data |
| Chemical formula |
C17H17NO4
|
|
M
r
|
299.31 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
6.9956 (5), 8.8589 (6), 12.0938 (9) |
| α, β, γ (°) |
93.980 (6), 106.603 (7), 102.133 (6) |
|
V (Å3) |
695.46 (9) |
|
Z
|
2 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.84 |
| Crystal size (mm) |
0.18 × 0.06 × 0.04 |
| |
| Data collection |
| Diffractometer |
Oxford Diffraction Gemini |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2015 ▸) |
|
T
min, T
max
|
0.818, 1 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
5235, 2456, 2147 |
|
R
int
|
0.027 |
| (sin θ/λ)max (Å−1) |
0.598 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.041, 0.121, 1.07 |
| No. of reflections |
2456 |
| No. of parameters |
202 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.22, −0.25 |
