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. 2017 Feb 21;73(Pt 3):130–137. doi: 10.1107/S2053230X17001911

Table 3. Data-collection and processing statistics.

Values in parentheses are for the outer shell.

Diffraction source BL41XU, SPring-8
Wavelength (Å) 1.0000
Temperature (K) 100
Detector PILATUS 6M
Crystal-to-detector distance (mm) 380
Rotation range per image (°) 0.5
Total rotation range (°) 180
Exposure time per image (s) 0.5
Space group C2
a, b, c (Å) 113.4, 44.6, 63.6
α, β, γ (°) 90, 120.3, 90
Matthews coefficient (V M) (Å3 Da−1) 2.07
Mosaicity (°) 0.34
Resolution range (Å) 50.00–1.90 (1.93–1.90)
Total No. of reflections 71783
No. of unique reflections 21371
Completeness (%) 98.1 (87.6)
Multiplicity 3.4 (2.8)
I/σ(I)〉 20.2 (2.0)
R meas 0.060 (0.436)
Overall B factor from Wilson plot (Å2) 28.7

R meas = Inline graphic Inline graphic.