Table 3. Data-collection and processing statistics.
Diffraction source | BL41XU, SPring-8 |
Wavelength (Å) | 1.0000 |
Temperature (K) | 100 |
Detector | PILATUS 6M |
Crystal-to-detector distance (mm) | 380 |
Rotation range per image (°) | 0.5 |
Total rotation range (°) | 180 |
Exposure time per image (s) | 0.5 |
Space group | C2 |
a, b, c (Å) | 113.4, 44.6, 63.6 |
α, β, γ (°) | 90, 120.3, 90 |
Matthews coefficient (V M) (Å3 Da−1) | 2.07 |
Mosaicity (°) | 0.34 |
Resolution range (Å) | 50.00–1.90 (1.93–1.90) |
Total No. of reflections | 71783 |
No. of unique reflections | 21371 |
Completeness (%) | 98.1 (87.6) |
Multiplicity | 3.4 (2.8) |
〈I/σ(I)〉 | 20.2 (2.0) |
R meas † | 0.060 (0.436) |
Overall B factor from Wilson plot (Å2) | 28.7 |
R meas = .