Table 7. . Stability of enalaprilat under different storage conditions (n = 6).
Serial number | Storage conditions | QC samples (ng/ml) | Mean (ng/ml) | SD | CV (%) | Accuracy (%) |
---|---|---|---|---|---|---|
1 | Autosampler stability 24 h at 24°C | 3 | 2.6650 | 0.2892 | 10.8514 | 98.5516 |
200 | 187.7900 | 31.1432 | 16.5840 | 93.8950 | ||
|
|
400 |
365.4017 |
18.0123 |
4.9295 |
92.5255 |
2 | Freeze and thaw stability at -20°C (3 cycles) | 3 | 2.3750 | 0.5358 | 22.5595 | 87.8274 |
200 | 177.4900 | 18.3801 | 10.3556 | 95.3222 | ||
|
|
400 |
348.4317 |
61.8666 |
17.7557 |
88.2284 |
3 | Bench top stability for 8 h | 3 | 2.8833 | 0.3502 | 12.1460 | 106.6256 |
200 | 190.4450 | 22.0556 | 11.5811 | 102.2798 | ||
|
|
400 |
387.3033 |
20.70389 |
5.3457 |
98.0713 |
4 | Long-term stability at -20.0°C for 30 days | 3 | 2.4967 | 0.4318 | 17.2939 | 92.3267 |
200 | 196.7650 | 8.2097 | 4.1723 | 105.6740 | ||
400 | 394.0400 | 12.4395 | 3.1569 | 99.7772 |