Table 2. 13C NMR spectral data of compounds 1−5 in CDCl3.
1 | 2 | 3 | 4 | 5 | |
---|---|---|---|---|---|
1 | 36.6 | 35.0 | 36.5 | 35.4 | 36.6 |
2 | 34.9 | 27.7 | 34.7 | 34.4 | 34.8 |
3 | 216.6 | 78.5 | 216.4 | 215.0 | 216.9 |
4 | 47.5 | 38.6 | 47.4 | 47.2 | 47.4 |
5 | 50.3 | 48.2 | 50.4 | 49.7 | 50.5 |
6 | 23.8 | 24.0 | 23.5 | 37.2 | 23.7 |
7 | 119.8 | 76.1 | 124.1 | 198.0 | 119.8 |
8 | 142.9 | 135.7 | 142.2 | 139.6 | 142.9 |
9 | 144.5 | 139.5 | 149.9 | 162.8 | 144.5 |
10 | 37.3 | 37.5 | 38.5 | 39.3 | 37.3 |
11 | 117.3 | 21.5 | 118.2 | 23.8 | 117.3 |
12 | 37.8 | 30.2 | 79.2 | 30.2 | 37.8 |
13 | 43.8 | 45.0 | 49.0 | 45.0 | 43.8 |
14 | 50.7 | 49.7 | 52.9 | 51.5 | 52.1 |
15 | 31.5 | 31.8 | 31.0 | 73.4 | 74.2 |
16 | 27.9 | 28.5 | 27.0 | 39.7 | 40.3 |
17 | 51.0 | 49.6 | 52.5 | 50.5 | 50.2 |
18 | 15.7 | 16.3 | 11.7 | 15.9 | 15.7 |
19 | 22.5 | 17.5 | 21.7 | 17.9 | 22.5 |
20 | 36.5 | 36.4 | 35.6 | 36.2 | 36.4 |
21 | 18.6 | 18.5 | 18.4 | 18.4 | 18.6 |
22 | 31.4 | 34.5 | 34.7 | 34.7 | 34.4 |
23 | 28.9 | 28.8 | 28.7 | 28.7 | 28.9 |
24 | 70.9 | 79.5 | 79.7 | 79.7 | 79.3 |
25 | 74.9 | 73.5 | 74.5 | 73.7 | 73.8 |
26 | 62.2 | 67.7 | 26.5 | 26.5 | 67.9 |
27 | 62.8 | 22.2 | 23.2 | 23.2 | 22.0 |
28 | 25.4 | 27.4 | 27.6 | 27.6 | 25.4 |
29 | 25.3 | 15.4 | 20.2 | 20.2 | 21.2 |
30 | 21.2 | 25.2 | 25.5 | 25.5 | 25.3 |
-OCH3 | 55.5 | 55.8 |