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Control experiments. (a) Stoichiometric reaction of [(cod)IrCl]2 with 2-MePy. (b) Stoichiometric reaction of [(cod)IrCl]2 with 2-MePy and o-carborane (1a). (c) Stoichiometric reaction of [(cod)IrCl]2 with 2-MePy and B2pin2. (d) Stoichiometric reaction of [(cod)IrCl]2 with 2-MePy and HBpin. (e) Standard catalytic borylation reaction of 1a monitored by 1H and 11B NMR. (f) (η6-MesH)Ir(Bpin)3 catalysed borylation reaction of 1a.
