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. 2017 Mar 17;8:14679. doi: 10.1038/ncomms14679

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Copyright © 2017, The Author(s)

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(a) The integrated detector counting rates as a function of temperature. The simultaneous DSC scan is superimposed, which shows a T_C∼594 K at a heating rate of 2.5 K min⁻¹. The coexistence of two phases can be clearly seen in the vicinity of T_C. (b) Full-Q range SANS data for three samples: as-cast condition (C), quenched from 623 K after the transformation had ended (S1), and quenched after crystallization at 673 K (X). The nearly complete overlap of the SANS profiles between the as-cast and S1 samples demonstrates the reentrant behaviour.