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. 2017 Feb 21;56(11):1585–1595. doi: 10.1021/acs.biochem.7b00056

Table 1.

time (min) % A (H2O with formic acid) % B (ACN with formic acid)
0.0 98.0 2.0
1.0 98.0 2.0
2.0 5.0 95.0
15.0 5.0 95.0