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. Author manuscript; available in PMC: 2017 Jun 5.
Published in final edited form as: Inorg Chem. 2016 Nov 15;55(23):12391–12399. doi: 10.1021/acs.inorgchem.6b02288

Figure 1.

Figure 1

(a) ORTEP plot of [CoII(Me3-TPADP)(CH3CN)2]2+ (1A) with thermal ellipsoid drawn at the 30 % probability level. Hydrogen atoms are omitted for clarity. Selected bond lengths (Å): Co1-N1 2.0574(14), Co1-N2 2.1999(14), Co1-N3 2.2108(14), Co1-N4 2.2050(14), Co1-N5 2.0514(15), Co1-N6 2.1151(15) (b) X-band EPR spectrum of 1 in frozen CH3CN at 5 K. Spectroscopic settings: frequency = 9.646 GHz, microwave power = 0.998 mW, modulation frequency = 100 kHz, and modulation amplitude = 1 mT.