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1H NMR spectra of (a) organic (toluene-d8) layer of TOAB (2.0 mmol) after mixing with the aqueous (D2O) layer of H2PtCl6 (0.4 mmol). (b) 1-Octanethiol (1.6 mmol) added to (a). (c) NaBH4 (4.0 mmol) added to (b). (d) S-Octylthiosulfate (0.8 mmol) added to (a). (e) Pt-SC8 in CDCl3 isolated after the reduction by NaBH4 of the solution (d). The peak at δ 2.10 ppm corresponds to the toluene solvent peak.
