Table 1.
Nuclear Magnetic Resonance (NMR) spectral data for compound 1 in CD3OD.
| Position | δC | δH (J in Hz) |
|---|---|---|
| 1 | 177.3, C | |
| 2 | 35.2, CH2 | 2.31, m |
| 3 | 24.2, CH2 | 2.33, m |
| 4 | 131.1, CH | 5.46, m |
| 5 | 127.6, CH | 5.47, m |
| 6 | 36.3, CH2 | 2.31, m |
| 7 | 73.0, CH | 4.10, dt (6.1, 6.1) |
| 8 | 136.2, CH | 5.72, dd (15.7, 6.1) |
| 9 | 130.9, CH | 5.78, dd (15.7, 6.1) |
| 10 | 76.0, CH | 3.96, dd (6.1, 4.7) |
| 11 | 75.9, CH | 3.53, dt (8.3, 4.7) |
| 12 | 31.8, CH2 | 2.18, dd (14.9, 8.3); 2.33, m |
| 13 | 127.4, CH | 5.49, m |
| 14 | 130.7, CH | 5.42, m |
| 15 | 26.8, CH2 | 2.84, dd (6.6, 6.1) |
| 16 | 129.0, CH | 5.34, m |
| 17 | 129.5, CH | 5.34, m |
| 18 | 26.4, CH2 | 2.81, dd (7.1, 5.9) |
| 19 | 128.2, CH | 5.29, m |
| 20 | 132.8, CH | 5.37, m |
| 21 | 21.5, CH2 | 2.08, q (7.3) |
| 22 | 14.7, CH3 | 0.96, t (7.6) |