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. 2017 Mar 28;12(3):e0173949. doi: 10.1371/journal.pone.0173949

Table 3. Effect of autoclaving sterilization on physicochemical properties of APS in-situ gels.

Lot number T sol-gel (°C) sol-geltransition time(s,37°C) pH %LA Viscosity (mpa∙s, 25°C)
Before autoclaving 01 34.1 ± 0.2 10.3 ± 0.1 6.5 101.1 ± 0.9 56.8 ± 1.2
02 33.6 ± 0.4 9.7 ± 0.1 6.4 100.5 ± 0.7 57.2 ± 1.3
03 34.3 ± 0.3 10.6 ± 0.2 6.5 101.6 ± 1.1 55.9 ± 0.7
After autoclaving 01 33.9 ± 0.3 9.9 ± 0.1 6.4 100.8 ± 1.2 57.2 ± 1.0
02 33.7 ± 0.5 9.6 ± 0.1 6.3 101.1 ± 0.9 56.6 ± 0.8
03 34.1 ± 0.2 10.4 ± 0.1 6.4 102.0 ± 0.7 56.1 ± 0.9

(n = 3, mean ± SD), % LA = labeled amount of APS, calculated based on glucose (C6H12O4), T sol-gel = sol-gel transition temperature.