Table 3. Effect of autoclaving sterilization on physicochemical properties of APS in-situ gels.
Lot number | T sol-gel (°C) | sol-geltransition time(s,37°C) | pH | %LA | Viscosity (mpa∙s, 25°C) | |
---|---|---|---|---|---|---|
Before autoclaving | 01 | 34.1 ± 0.2 | 10.3 ± 0.1 | 6.5 | 101.1 ± 0.9 | 56.8 ± 1.2 |
02 | 33.6 ± 0.4 | 9.7 ± 0.1 | 6.4 | 100.5 ± 0.7 | 57.2 ± 1.3 | |
03 | 34.3 ± 0.3 | 10.6 ± 0.2 | 6.5 | 101.6 ± 1.1 | 55.9 ± 0.7 | |
After autoclaving | 01 | 33.9 ± 0.3 | 9.9 ± 0.1 | 6.4 | 100.8 ± 1.2 | 57.2 ± 1.0 |
02 | 33.7 ± 0.5 | 9.6 ± 0.1 | 6.3 | 101.1 ± 0.9 | 56.6 ± 0.8 | |
03 | 34.1 ± 0.2 | 10.4 ± 0.1 | 6.4 | 102.0 ± 0.7 | 56.1 ± 0.9 |
(n = 3, mean ± SD), % LA = labeled amount of APS, calculated based on glucose (C6H12O4), T sol-gel = sol-gel transition temperature.