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. 2017 Mar 16;9(3):106. doi: 10.3390/toxins9030106

Table 3.

Multiple reaction monitoring (MRM) parameters for detection of 13 mycotoxins by the mass spectrometer.

Mycotoxin Precursor ion Q1 (m/z) Q3 (m/z) Time (msec) DP (volts) EP (volts) CE (volts) CXP (volts)
NIV [M + CH3COO−]− 313
313		 175
295		 100
100		 41
41		 5
5		 19
15		 6
6
DON [M + CH3COO−]− 297.2
297.2		 249.2
231.2		 100
100		 40
40		 7.5
7.5		 12
12		 4
4
3-AcDON [M + CH3COO−]− 339
339		 231
213		 100
100		 15
15		 3.5
3.5		 15
15		 2
2
AFB1 [M + H]+ 313
313		 285.1
115		 100
100		 70
70		 11
11		 51
89		 4
4
AFB2 [M + H]+ 313
313		 287.1
259.1		 100
100		 70
70		 10
10		 50
50		 3
3
AFG1 [M + H]+ 329
329		 243.0
215.1		 100
100		 70
70		 11
10		 25
50		 4
4
AFG2 [M + H]+ 331
331		 189
257		 100
100		 70
70		 10.0
10.5		 50
47		 3
4
FB1 [M + H]+ 722.4
722.4		 334.3
352.4		 100
100		 91
91		 8
8		 53
43		 6
6
FB2 [M + H]+ 706.4
706.4		 336.4
318.2		 100
100		 70
70		 9
9		 45
47		 6
6
HT-2 [M + NH4]+ 442
442		 263
215		 100
100		 26
26		 3
3		 19
19		 4
4
T-2 [M + NH4]+ 484.1
484.1 		215.2
185.2 		100
100 		21
21 		6
6 		29
31 		4
4
ZEN [M − H]− 317.1
317.1		 131
175		 100
100		 −50
−50		 −4.5
−4.5		 −40
−34		 −2
−2
OTA [M + H]+ 404
404		 239
220.9		 100
100		 41
41		 5
5		 31
19		 4
4