Table 1.
Atom No. | 13C NMR | 1H NMR |
---|---|---|
1 | 40.7 | 0.75 m, 1.86 m |
2 | 20.1 | 1.36 m, 2.29 m |
3 | 38.9 | 1.01 m, 2.30 m |
4 | 44.7 | - |
5 | 57.9 | 1.05 d (13.1) |
6 | 23.9 | 2.23 m, 2.39 m |
7 | 43.0 | 1.40 m, 1.80 m |
8 | 41.6 | - |
9 | 54.8 | 0.91 d (7.9) |
10 | 40.2 | - |
11 | 20.6 | 1.68 m, 1.88 m |
12 | 39.0 | 1.95 m, 2.69 m |
13 | 88.0 | - |
14 | 43.9 | 1.99 m, 2.74 d (10.6) |
15 | 46.9 | 1.87 m, 2.02 m |
16 | 153.7 | - |
17 | 105.4 | 4.89 bs, 5.71 bs |
18 | 28.7 | 1.33 s |
19 | 177.3 | - |
20 | 17.1 | 1.37 s |