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. 2017 Jan 31;7(1):10. doi: 10.3390/biom7010010

Table 1.

1H and 13C Nuclear Magnetic Resonance (NMR) (500 and 125 MHz, 300 K) assignments of the aglycone of compound (1) in pyridine-d5.

Atom No. 13C NMR 1H NMR
1 40.7 0.75 m, 1.86 m
2 20.1 1.36 m, 2.29 m
3 38.9 1.01 m, 2.30 m
4 44.7 -
5 57.9 1.05 d (13.1)
6 23.9 2.23 m, 2.39 m
7 43.0 1.40 m, 1.80 m
8 41.6 -
9 54.8 0.91 d (7.9)
10 40.2 -
11 20.6 1.68 m, 1.88 m
12 39.0 1.95 m, 2.69 m
13 88.0 -
14 43.9 1.99 m, 2.74 d (10.6)
15 46.9 1.87 m, 2.02 m
16 153.7 -
17 105.4 4.89 bs, 5.71 bs
18 28.7 1.33 s
19 177.3 -
20 17.1 1.37 s