Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C15H15NOS |
| M r | 257.34 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 120 |
| a, b, c (Å) | 6.2405 (4), 9.9975 (6), 20.7815 (13) |
| β (°) | 93.097 (2) |
| V (Å3) | 1294.65 (14) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.24 |
| Crystal size (mm) | 0.53 × 0.16 × 0.09 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD area detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2014 ▸) |
| T min, T max | 0.885, 0.979 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 50820, 3381, 3116 |
| R int | 0.031 |
| (sin θ/λ)max (Å−1) | 0.677 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.068, 0.182, 1.14 |
| No. of reflections | 3381 |
| No. of parameters | 166 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.16, −0.81 |
Computer programs: APEX2 and SAINT (Bruker, 2014 ▸), SHELXS97 (Sheldrick, 2008 ▸), SHELXL2016 (Sheldrick, 2015 ▸), WinGX (Farrugia, 2012 ▸), DIAMOND (Brandenburg, 2006 ▸), GOLD (Chen et al., 2015 ▸), Crystal Explorer (Wolff et al., 2012 ▸), publCIF (Westrip, 2010 ▸) and enCIFer (Allen et al., 2004 ▸).