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. 2017 Mar 14;73(Pt 4):503–506. doi: 10.1107/S2056989017003607
O1—C1 1.357 (8) C9—H9 0.9800
O1—C7 1.439 (8) C11—C18 1.508 (9)
O2—C8 1.215 (6) C11—C12 1.518 (9)
O3—C10 1.238 (6) C11—H11 0.9800
O4—C21 1.282 (9) C12—C17 1.371 (9)
O4—C22 1.461 (8) C12—C13 1.379 (10)
O5—C21 1.151 (8) C13—C14 1.369 (11)
N1—C10 1.314 (7) C13—H13 0.9300
N1—C11 1.461 (7) C14—C15 1.364 (12)
N1—H1 0.8600 C14—H14 0.9300
C1—C2 1.373 (9) C15—C16 1.346 (11)
C1—C6 1.378 (9) C15—H15 0.9300
C2—C3 1.398 (8) C16—C17 1.369 (10)
C2—H2 0.9300 C16—H16 0.9300
C3—C4 1.380 (8) C17—H17 0.9300
C3—H3 0.9300 C18—H18A 0.9600
C4—C5 1.386 (8) C18—H18B 0.9600
C4—C8 1.481 (8) C18—H18C 0.9600
C5—C6 1.374 (9) C19—C20 1.515 (8)
C5—H5 0.9300 C19—H19A 0.9700
C6—H6 0.9300 C19—H19B 0.9700
C7—H7A 0.9600 C20—C21 1.498 (9)
C7—H7B 0.9600 C20—H20A 0.9700
C7—H7C 0.9600 C20—H20B 0.9700
C8—C9 1.509 (8) C22—H22A 0.9600
C9—C10 1.519 (8) C22—H22B 0.9600
C9—C19 1.542 (8) C22—H22C 0.9600
C1—O1—C7 117.6 (6) C12—C11—H11 107.4
C21—O4—C22 115.9 (7) C17—C12—C13 117.3 (7)
C10—N1—C11 123.7 (5) C17—C12—C11 122.6 (7)
C10—N1—H1 118.1 C13—C12—C11 120.1 (7)
C11—N1—H1 118.1 C14—C13—C12 121.3 (8)
O1—C1—C2 123.9 (7) C14—C13—H13 119.4
O1—C1—C6 116.3 (7) C12—C13—H13 119.4
C2—C1—C6 119.8 (7) C15—C14—C13 119.8 (9)
C1—C2—C3 118.7 (7) C15—C14—H14 120.1
C1—C2—H2 120.6 C13—C14—H14 120.1
C3—C2—H2 120.6 C16—C15—C14 120.0 (10)
C4—C3—C2 122.2 (6) C16—C15—H15 120.0
C4—C3—H3 118.9 C14—C15—H15 120.0
C2—C3—H3 118.9 C15—C16—C17 120.3 (9)
C3—C4—C5 117.5 (6) C15—C16—H16 119.9
C3—C4—C8 117.9 (6) C17—C16—H16 119.9
C5—C4—C8 124.6 (6) C16—C17—C12 121.4 (8)
C6—C5—C4 121.0 (7) C16—C17—H17 119.3
C6—C5—H5 119.5 C12—C17—H17 119.3
C4—C5—H5 119.5 C11—C18—H18A 109.5
C5—C6—C1 120.8 (7) C11—C18—H18B 109.5
C5—C6—H6 119.6 H18A—C18—H18B 109.5
C1—C6—H6 119.6 C11—C18—H18C 109.5
O1—C7—H7A 109.5 H18A—C18—H18C 109.5
O1—C7—H7B 109.5 H18B—C18—H18C 109.5
H7A—C7—H7B 109.5 C20—C19—C9 114.2 (5)
O1—C7—H7C 109.5 C20—C19—H19A 108.7
H7A—C7—H7C 109.5 C9—C19—H19A 108.7
H7B—C7—H7C 109.5 C20—C19—H19B 108.7
O2—C8—C4 121.0 (6) C9—C19—H19B 108.7
O2—C8—C9 121.2 (6) H19A—C19—H19B 107.6
C4—C8—C9 117.8 (5) C21—C20—C19 112.2 (6)
C8—C9—C10 109.7 (5) C21—C20—H20A 109.2
C8—C9—C19 113.3 (5) C19—C20—H20A 109.2
C10—C9—C19 107.5 (5) C21—C20—H20B 109.2
C8—C9—H9 108.7 C19—C20—H20B 109.2
C10—C9—H9 108.7 H20A—C20—H20B 107.9
C19—C9—H9 108.7 O5—C21—O4 121.9 (9)
O3—C10—N1 123.6 (6) O5—C21—C20 125.6 (9)
O3—C10—C9 119.7 (6) O4—C21—C20 112.5 (7)
N1—C10—C9 116.7 (5) O4—C22—H22A 109.5
N1—C11—C18 110.0 (6) O4—C22—H22B 109.5
N1—C11—C12 109.0 (5) H22A—C22—H22B 109.5
C18—C11—C12 115.3 (6) O4—C22—H22C 109.5
N1—C11—H11 107.4 H22A—C22—H22C 109.5
C18—C11—H11 107.4 H22B—C22—H22C 109.5