| Nonius Kappa CCD diffractometer | 5119 reflections with I > 2σ(I) |
| θ/2θ scans | Rint = 0.031 |
| Absorption correction: ψ scan (North et al., 1968) | θmax = 31.1°, θmin = 3.0° |
| Tmin = 0.856, Tmax = 0.919 | h = −22→22 |
| 29723 measured reflections | k = −12→11 |
| 6435 independent reflections | l = −21→22 |