Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C24H19N3O5S |
| M r | 461.48 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 173 |
| a, b, c (Å) | 15.6096 (4), 8.8817 (2), 15.8973 (4) |
| β (°) | 98.601 (2) |
| V (Å3) | 2179.21 (9) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.19 |
| Crystal size (mm) | 0.58 × 0.21 × 0.20 |
| Data collection | |
| Diffractometer | Nonius Kappa CCD |
| Absorption correction | ψ scan (North et al., 1968 ▸) |
| T min, T max | 0.856, 0.919 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 29723, 6435, 5119 |
| R int | 0.031 |
| (sin θ/λ)max (Å−1) | 0.727 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.041, 0.107, 1.03 |
| No. of reflections | 6435 |
| No. of parameters | 300 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.43, −0.29 |