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. 2017 Mar 14;73(Pt 4):515–519. doi: 10.1107/S2056989017003541
O1—C2 1.3747 (16) C11—H11 0.9500
O1—C5 1.3796 (15) C12—C15 1.5247 (19)
N1—C1 1.5007 (16) C12—C14 1.5259 (18)
N1—C12 1.5198 (16) C12—C13 1.5279 (18)
N1—H1A 0.968 (15) C13—H13A 0.9800
N1—H1B 0.936 (15) C13—H13B 0.9800
C1—C2 1.4817 (18) C13—H13C 0.9800
C1—H1C 0.9900 C14—H14A 0.9800
C1—H1D 0.9900 C14—H14B 0.9800
C2—C3 1.352 (2) C14—H14C 0.9800
C3—C4 1.424 (2) C15—H15A 0.9800
C3—H3 0.9500 C15—H15B 0.9800
C4—C5 1.353 (2) C15—H15C 0.9800
C4—H4 0.9500 O2—C16 1.2351 (17)
C5—C6 1.4609 (19) O3—C16 1.2866 (17)
C6—C7 1.396 (2) O3—H5O 1.257 (17)
C6—C11 1.4022 (19) O4—C19 1.2300 (16)
C7—C8 1.387 (2) O5—C19 1.2979 (16)
C7—H7 0.9500 O5—H5O 1.160 (17)
C8—C9 1.388 (2) C16—C17 1.4947 (19)
C8—H8 0.9500 C17—C18 1.3343 (18)
C9—C10 1.387 (2) C17—H17 0.9500
C9—H9 0.9500 C18—C19 1.4952 (18)
C10—C11 1.384 (2) C18—H18 0.9500
C10—H10 0.9500
C2—O1—C5 106.85 (10) C10—C11—H11 119.7
C1—N1—C12 117.49 (10) C6—C11—H11 119.7
C1—N1—H1A 108.0 (8) N1—C12—C15 108.92 (10)
C12—N1—H1A 108.0 (8) N1—C12—C14 109.41 (11)
C1—N1—H1B 109.6 (9) C15—C12—C14 111.64 (11)
C12—N1—H1B 106.5 (9) N1—C12—C13 105.08 (10)
H1A—N1—H1B 106.6 (12) C15—C12—C13 111.28 (11)
C2—C1—N1 111.02 (10) C14—C12—C13 110.29 (11)
C2—C1—H1C 109.4 C12—C13—H13A 109.5
N1—C1—H1C 109.4 C12—C13—H13B 109.5
C2—C1—H1D 109.4 H13A—C13—H13B 109.5
N1—C1—H1D 109.4 C12—C13—H13C 109.5
H1C—C1—H1D 108.0 H13A—C13—H13C 109.5
C3—C2—O1 109.83 (12) H13B—C13—H13C 109.5
C3—C2—C1 134.49 (13) C12—C14—H14A 109.5
O1—C2—C1 115.65 (12) C12—C14—H14B 109.5
C2—C3—C4 106.78 (13) H14A—C14—H14B 109.5
C2—C3—H3 126.6 C12—C14—H14C 109.5
C4—C3—H3 126.6 H14A—C14—H14C 109.5
C5—C4—C3 107.10 (12) H14B—C14—H14C 109.5
C5—C4—H4 126.4 C12—C15—H15A 109.5
C3—C4—H4 126.4 C12—C15—H15B 109.5
C4—C5—O1 109.43 (12) H15A—C15—H15B 109.5
C4—C5—C6 134.61 (13) C12—C15—H15C 109.5
O1—C5—C6 115.96 (12) H15A—C15—H15C 109.5
C7—C6—C11 118.51 (13) H15B—C15—H15C 109.5
C7—C6—C5 121.38 (12) C16—O3—H5O 111.3 (7)
C11—C6—C5 120.11 (13) C19—O5—H5O 111.7 (8)
C8—C7—C6 120.65 (13) O2—C16—O3 123.38 (13)
C8—C7—H7 119.7 O2—C16—C17 116.77 (12)
C6—C7—H7 119.7 O3—C16—C17 119.85 (12)
C7—C8—C9 120.20 (15) C18—C17—C16 130.78 (13)
C7—C8—H8 119.9 C18—C17—H17 114.6
C9—C8—H8 119.9 C16—C17—H17 114.6
C10—C9—C8 119.80 (14) C17—C18—C19 130.28 (12)
C10—C9—H9 120.1 C17—C18—H18 114.9
C8—C9—H9 120.1 C19—C18—H18 114.9
C11—C10—C9 120.17 (13) O4—C19—O5 123.00 (12)
C11—C10—H10 119.9 O4—C19—C18 117.33 (12)
C9—C10—H10 119.9 O5—C19—C18 119.67 (12)
C10—C11—C6 120.67 (14)
C12—N1—C1—C2 −172.59 (11) C11—C6—C7—C8 0.0 (2)
C5—O1—C2—C3 0.25 (14) C5—C6—C7—C8 179.45 (13)
C5—O1—C2—C1 178.57 (11) C6—C7—C8—C9 −0.6 (2)
N1—C1—C2—C3 −109.20 (17) C7—C8—C9—C10 0.4 (2)
N1—C1—C2—O1 73.02 (14) C8—C9—C10—C11 0.3 (2)
O1—C2—C3—C4 0.17 (15) C9—C10—C11—C6 −0.9 (2)
C1—C2—C3—C4 −177.70 (14) C7—C6—C11—C10 0.8 (2)
C2—C3—C4—C5 −0.53 (16) C5—C6—C11—C10 −178.73 (12)
C3—C4—C5—O1 0.70 (16) C1—N1—C12—C15 67.55 (14)
C3—C4—C5—C6 −178.87 (14) C1—N1—C12—C14 −54.73 (14)
C2—O1—C5—C4 −0.60 (14) C1—N1—C12—C13 −173.13 (11)
C2—O1—C5—C6 179.06 (11) O2—C16—C17—C18 −172.20 (14)
C4—C5—C6—C7 −179.94 (15) O3—C16—C17—C18 7.4 (2)
O1—C5—C6—C7 0.51 (18) C16—C17—C18—C19 −1.3 (3)
C4—C5—C6—C11 −0.5 (2) C17—C18—C19—O4 176.22 (14)
O1—C5—C6—C11 179.98 (11) C17—C18—C19—O5 −3.2 (2)