| Bruker APEXII CCD diffractometer | Rint = 0.075 |
| φ and ω scans | θmax = 28.7°, θmin = 2.4° |
| 14119 measured reflections | h = −5→7 |
| 2813 independent reflections | k = −23→23 |
| 1889 reflections with I > 2σ(I) | l = −15→14 |
| Bruker APEXII CCD diffractometer | Rint = 0.075 |
| φ and ω scans | θmax = 28.7°, θmin = 2.4° |
| 14119 measured reflections | h = −5→7 |
| 2813 independent reflections | k = −23→23 |
| 1889 reflections with I > 2σ(I) | l = −15→14 |