| Bruker D8 QUEST ECO diffractometer | 1203 independent reflections |
| Radiation source: sealed tube, Siemens KFFMO2K-90C | 1070 reflections with I > 2σ(I) |
| Curved graphite monochromator | Rint = 0.033 |
| Detector resolution: 8.3660 pixels mm-1 | θmax = 26.8°, θmin = 2.5° |
| ω and φ scans | h = −21→21 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −10→10 |
| Tmin = 0.47, Tmax = 0.64 | l = −10→10 |
| 4708 measured reflections |