Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C14H8Br2 |
| M r | 336.02 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 173 |
| a, b, c (Å) | 16.840 (3), 8.6112 (16), 8.1418 (15) |
| β (°) | 103.735 (2) |
| V (Å3) | 1146.9 (4) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 7.03 |
| Crystal size (mm) | 0.25 × 0.11 × 0.07 |
| Data collection | |
| Diffractometer | Bruker D8 QUEST ECO |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.47, 0.64 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 4708, 1203, 1070 |
| R int | 0.033 |
| (sin θ/λ)max (Å−1) | 0.634 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.030, 0.083, 1.06 |
| No. of reflections | 1203 |
| No. of parameters | 73 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.01, −0.35 |