| Agilent SuperNova, Dual, Cu at zero, Atlas diffractometer | 3662 independent reflections |
| Radiation source: micro-source | 3405 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.036 |
| Detector resolution: 10.3953 pixels mm-1 | θmax = 26.6°, θmin = 1.4° |
| φ scans and ω scans with κ offset | h = −8→9 |
| Absorption correction: multi-scan (CrysAlisPro; Agilent, 2013) | k = −7→10 |
| Tmin = 0.300, Tmax = 1.000 | l = −18→18 |
| 7508 measured reflections |