Bruker APEXII CCD diffractometer | 3527 reflections with I > 2σ(I) |
φ and ω scans | Rint = 0.054 |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | θmax = 27.6°, θmin = 2.4° |
Tmin = 0.618, Tmax = 0.681 | h = −12→12 |
39878 measured reflections | k = −12→12 |
3616 independent reflections | l = −21→21 |