Table 2.
1-13C G | 2-13C G | 1-13C E | 2-13C E | 3-13C E | 4-13C E | |
---|---|---|---|---|---|---|
His CO | 31 | 7 | 1 | 0 | 0 | 3 |
His α | 3 | 40 | 1 | 1 | 24 | 1 |
His β | 0 | 0 | 9 | 34 | 1 | 0 |
His γ | n.d | n.d | n.d | n.d | n.d | n.d |
His δ2 | 26 | 52 | 4 | 4 | 3 | 2 |
His ε1 | 37 | 8 | 1 | 1 | 3 | 14 |
Values are in %. Errors are estimated to 1% for 1H bound 13C, 3% for others. 1% for non labeled positions is expected because of natural abundance of 13C