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. 2017 Feb 28;67(3):191–200. doi: 10.1007/s10858-017-0096-7

Table 2.

Site-selective 13C incorporation in histidine using glucose (G) or erythrose (E)

1-13C G 2-13C G 1-13C E 2-13C E 3-13C E 4-13C E
His CO 31 7 1 0 0 3
His α 3 40 1 1 24 1
His β 0 0 9 34 1 0
His γ n.d n.d n.d n.d n.d n.d
His δ2 26 52 4 4 3 2
His ε1 37 8 1 1 3 14

Values are in %. Errors are estimated to 1% for 1H bound 13C, 3% for others. 1% for non labeled positions is expected because of natural abundance of 13C