TABLE 1.
Data collection and refinement statistics
| ObgE_340 - GDP | |
|---|---|
| Data collection and processing | |
| X-ray source | SOLEIL PROXIMA II |
| Wavelength (Å) | 1.07812 |
| Resolution range (Å)a | 49.00–1.85 (1.90–1.85) |
| Total/unique reflections | 280,027/41,090 (20,519/1,943) |
| Rmeas (%) | 9.7 (182.3) |
| I/σI | 9.67 (1.00) |
| CC1/2 | 99.8 (48.9) |
| Completeness (%) | 99.9 (100) |
| Redundancy | 6.81 (6.97) |
| Space group | C2221 |
| Cell dimensions | |
| a, b, c (Å) | 64.6, 83.0, 177.4 |
| a, b, g (°) | 90, 90, 90 |
| Model refinement | |
| Rwork/Rfree (%)b | 19.8/23.9 |
| R.m.s. deviation bond length (Å) | 0.0154 |
| R.m.s. deviation bond angle (°) | 1.7629 |
| Ramachandran | |
| Favored/allowed/disallowed regions (%) | 98.5/0.9/0.6 |
| PDB code | 5M04 |
a Values for the highest-resolution shell are given in between brackets. CC1/2 values were used as a guide for selecting the highest usable resolution shell (67).
b A subset of 5% of the reflections was used for calculating Rfree.