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. 2017 Feb 21;409(12):3145–3151. doi: 10.1007/s00216-017-0255-4

Table 3.

Precision data (n = 5 for within-run precision; n = 3 for between-run precision) in spiked plasma samples

Analyte Precision (CV%)
At the LLOQ level Low, medium, and high concentration QC-s
Within-run Between-run Within-run Between-run
Spironolactone 8.9 7.9 3.2 2.7
7-Alpha-methylthiospironolactone 4.0 2.1 2.7 2.1
Canrenone 7.8 7.5 2.7 2.1

Quality control samples at low (4 ng/ml), medium (80 ng/ml), and high (220 ng/ml) concentration