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The XRD patters of the initial UOV and intermediates recovered after 5, 30, and 60 minutes of hydrolysis in 12 m HCl, together with the final material after treatment for 1 day. It is clear that the positions of those reflections with h=0 are approximately invariant during the process while those with h≠0 are significantly shifted, which is consistent with the predicted ADOR process for UOV shown in Figure 1.
