Table 2. Domain Spacings (L0) and Phase Characterizations of NDI-ODMS Conjugates of Family 1 and 2.
| compound | L0 (nm)a | phase |
|---|---|---|
| Si7-NDI-Si7 | 9.3 (A), 2.9 (B), 86.9° (γ) | Colob |
| Si7-NDI2-Si7 | 6.1 | Colh |
| Si15-NDI-Si15 | 6.5 | Colh |
| Si15-NDI2-Si15 | 7.4 | Colh |
| Si23-NDI-Si23 | 7.8 (A), 6.8 (B), 80° (γ) | Colobb |
| Si23-NDI2-Si23 | 8.8 | Colh |
| NDI-Si8-NDI | 4.4 | LAM |
| NDI2-Si8-NDI2 | 5.2 | LAM |
| NDI-Si16-NDI | 5.7 | LAM |
| NDI2-Si16-NDI2 | 6.3 | LAMc |
| NDI-Si24-NDI | 6.9 | LAMc |
| NDI2-Si24-NDI2 | 7.2 | LAMc |
a
L0 is the lattice parameter(s) in Colh and Colob and the bilayer thickness in LAM.
b
Measured at 5 °C.
c
Samples annealed for 30 min at 300 °C.