Skip to main content
. 2017 Apr 27;12(4):e0176550. doi: 10.1371/journal.pone.0176550

Table 1. Data collection and refinement statistics.

Data collection and Processing
    Wavelength (Å) 1.458
    Resolution range (Å) 44.61–2.39 (2.48–2.39)
    Space group P212121
    Unit cell (Å) a = 50.42, b = 76.37, c = 95.66
    Total reflections 78,940 (5,903)
    Unique reflections 14,895 (1,294)
    Multiplicity 5.3 (4.6)
    Completeness (%) 98.2 (87.7)
    Mean I/sigma(I) 7.03 (1.26)
    Wilson B-factor 44.9
    R-merge 0.159 (1.292)
    R-meas 0.176
    CC1/2 0.99 (0.61)
Refinement
    Rwork 0.2011 (0.3215)
    Rfree 0.2475 (0.3477)
    Protein residues 315
    Ligands 2 (PO4)
    Solvent molecules 51
    RMS(bonds) (Å) 0.009
    RMS(angles) (°) 1.18
    Ramachandran analysis (%)
      Favoured 95
      Allowed 5
      Outliers 0
    Average B-factor (Å2) 48.00