Table 3.
No. | 3 a | 4 a | 5 a | 6 a | 7 b |
---|---|---|---|---|---|
1 | 164.1, C | 78.2, C | 88.1, C | 89.6, C | 76.1, C |
2 | 119.3, CH | 131.8, CH | 128.7, CH | 129.8, CH | 134.6, CH |
3 | 136.6, CH | 134.9, CH | 139.8, CH | 139.9, CH | 132.4, CH |
4 | 121.7, C | 73.6, C | 73.5, C | 74.0, C | 75.2, CH |
5 | 187.7, C | 34.3, CH2 | 38.1, CH2 | 36.9, CH2 | 34.3, CH2 |
6 | 100.4, CH | 34.3, CH2 | 36.1, CH2 | 34.5, CH2 | 25.7, CH2 |
7 | 209.6, C | 212.0, C | 217.8, C | 215.1, C | 66.1, CH |
8 | 91.3, C | 88.1, C | 79.8, C | 90.0, C | 83.6, C |
9 | 40.5, CH2 | 37.4, CH2 | 42.1, CH2 | 36.7, CH2 | 34.8, CH2 |
10 | 25.8, CH2 | 24.8, CH2 | 25.9, CH2 | 27.5, CH2 | 27.4, CH2 |
11 | 152.1, CH | 133.8, CH | 150.9, CH | 80.8, CH | 141.0, CH |
12 | 130.1, C | 137.5, C | 125.2, C | 44.1, CH | 134.1, C |
13 | 36.5, CH2 | 26.5, CH2 | 25.1, CH2 | 17.9, CH2 | 31.0, CH2 |
14 | 31.6, CH2 | 33.0, CH2 | 29.1, CH2 | 28.2, CH2 | 39.7, CH2 |
15 | 38.6, CH | 38.8, CH | 38.3, CH | 38.0, CH | 36.3, CH |
16 | 21.8, CH3 | 18.1, CH3 | 17.5, CH3 | 17.6, CH3 | 17.2, CH3 |
17 | 21.4, CH3 | 17.0, CH3 | 16.9, CH3 | 17.0, CH3 | 16.0, CH3 |
18 | 12.2, CH3 | 31.4, CH3 | 26.9, CH3 | 24.4, CH3 | 33.5, CH3 |
19 | 20.9, CH3 | 28.0, CH3 | 28.3, CH3 | 24.0, CH3 | 21.6, CH3 |
20 | 169.2, C | 172.1, C | 168.9, C | 175.3, C | 168.4, C |
21 | 51.5, CH3 |
a in methanol-d4; b in CDCl3.