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. 2017 Mar 8;174(1):56–72. doi: 10.1104/pp.16.00055

Table I. 13C-NMR results for 1, 2, and 3.

Samples were analyzed at 300 K. The isolated product 1 was dissolved in MeCN-d3 (99.8 atom % D), while 2 and 3 were dissolved in CDCl3 (99.8 atom % D).

C 1 2 3

δC
δC
δC
1 128.7 148.7 147.2
2 26.4 110.9 111.2
3 40.6 116.4 114.4
4 137.7 143.5 144.6
5 127.1 54.8 51.9
6 79.3 81.2 81.2
7 46.2 40.6 37.2
8 23.7 18.6 18.9
9 37.7 37.6 32.1
10 139.4 39.0 37.7
11 41.5 41.3 40.6
12 180.6 179.3 178.9
13 10.9 9.2 10.2
14 22.2 18.6 25.5
15 17.4 26.0 26.1